The Shenzhen soil and remolded bentonite was prepared after drying with drying method and freeze dry method, with the cumulative intrusion curve obtained form mercury intrusion test, gave the division of pore scale for soil according to the test result. The difference of soil prepared by drying method in different temperature and freeze dry method was analyzed, and draw the conclusion that when drying for soil sample using in mercury intrusion test, the freeze dry method was better than drying method.